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Ajhil at 09:31, 31 August 2016

2016-08-31T09:31:22Z

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__NOTOC__
{{OR/15/070}}
==Blank data for detection limit and limit of quantification==

<center>
{| class="wikitable"
|+ Table 5    Blank raw data
|
| ! scope="col" style="width: 175px;" | '''[phytic acid] '''mg kg-1
|-
| ! scope="col" style="width: 175px;" | '''Blank 1'''
| 1034
|-
| '''Blank 2'''
| 772
|-
| '''Blank 3'''
| 912
|-
| '''Blank 4'''
| 981
|-
| '''Blank 5'''
| 1160
|-
| '''Blank 6'''
| 832
|-
| '''Blank 7'''
| 772
|-
| '''Blank 8'''
| 912
|-
| '''Blank 9'''
| 981
|-
| '''Blank 10'''
| 1160
|}
</center>

==Oat flour reference material raw data==

<center>
{| class="wikitable"
|+ Table 6    Oat flour reference material raw data
| ! scope="col" style="width: 175px;" | '''Oat Powder (g/100g)'''
| ! scope="col" style="width: 175px;" | '''Oat Powder (mg kg-1)'''
|-
| 1.8466
| 18466
|-
| 1.843
| 18430
|-
| 1.7794
| 17794
|-
| 1.6441
| 16441
|-
| 1.8179
| 18179
|}
</center>

==Standards at 7 and 80% of the top calibration standard raw data==

<center>
{| class="wikitable"
|+ Table 7    Standards at 7 and 80% of the top calibration standard raw data
|
| colspan="2" | '''5% standard'''
|-
| ! scope="col" style="width: 225px;" |
| ! scope="col" style="width: 175px;" | Phosphorus
| ! scope="col" style="width: 175px;" | Phytic acid
|-
| Target Value (mg kg-1)
| 517
| 1790
|-
| Mean measurement (mg kg-1)
| 474
| 1679
|-
| Accuracy
| 92%
| 94%
|-
| Measured SD (mg kg-1)
| 34
| 122
|-
| Precision (%RSD)
| 7.2
| 7.2
|}
</center>

<center>
{| class="wikitable"
|
| colspan="2" | '''80% standard'''
|-
| ! scope="col" style="width: 200px;" |
| ! scope="col" style="width: 175px;" | Phosphorus
| ! scope="col" style="width: 175px;" | Phytic acid
|-
| Target Value (mg kg-1)
| 6000
| 23679
|-
| Mean measurement (mg kg-1)
| 5970
| 21233
|-
| Accuracy
| 99%
| 90%
|-
| Measured SD (mg kg-1)
| 298
| 902
|-
| Precision (%RSD)
| 5.0
| 4.2
|}
</center>

==All rice and grain sample raw data==

<center>
{| class="wikitable"
|+ Table 8    All rice and grain sample raw data
| ! scope="col" style="width: 100px;" |
| ! scope="col" style="width: 100px;" | '''Run 1'''
| ! scope="col" style="width: 100px;" | '''Run 2'''
| ! scope="col" style="width: 100px;" | '''Run 3'''
| ! scope="col" style="width: 100px;" | '''Run 4'''
| ! scope="col" style="width: 100px;" | '''Run 5'''
|-
|
| colspan="5" | '''Phytate (mg kg-1)'''
|-
| '''Rice 1'''
| 6383
| 6619
| 6587
| '''NA'''
| 6311
|-
| '''Rice 1'''
| 6430
| 6371
| 5849
| '''NA'''
| 6215
|-
| '''Rice 1'''
| 6616
| 6343
| 6932
| '''NA'''
| 6650
|-
| '''Rice 2'''
| 1463
| 1856
| 1121
| 1301
| 1796
|-
| '''Rice 2'''
| 1826
| 1963
| 1285
| 1274
| 1632
|-
| '''Rice 2'''
| 1585
| 1743
| 1364
| 1033
| 1775
|-
| '''Grain 1'''
| 9688
| 12274
| 11998
| 9628
| 11069
|-
| '''Grain 1'''
| 9784
| 12772
| 11533
| 10831
| 10709
|-
| '''Grain 1'''
| 9953
| 12373
| 9159
| 11097
| 11587
|-
| '''Grain 2'''
| 9272
| 10337
| 8748
| 10921
| 9433
|-
| '''Grain 2'''
| 9629
| 10235
| 9209
| 11569
| 9878
|-
| '''Grain 2'''
| 8984
| 9799
| 9161
| 8675
| 11285
|}
</center>

<center>
{| class="wikitable"
|+ Table 9    Spike recovery raw data
| ! scope="col" style="width: 200px;" |
| ! scope="col" style="width: 175px;" | '''Phytic acid'''
|-
| Target Value (mg kg-1)
| 9090
|-
| Mean Measurement (mg kg-1)
| 8550
|-
| Average Recovery (%)
| 94
|-
| Measured SD
| 65
|-
| Precision (%RSD)
| 0.8
|}
</center>

==Analyst variation raw data==
<center>
{| class="wikitable"
|+ Table 10    Analyst variation raw data
| '''ADZ lentils [Phytic acid mg kg-1]'''
| '''DR Lentils [Phytic acid mg kg-1]'''
|- style="text-align:center;"
| 6762
| 6129
|- style="text-align:center;"
| 7791
| 7791
|- style="text-align:center;"
| 6310
| 6310
|- style="text-align:center;"
| 8173
| 6762
|- style="text-align:center;"
|
| 7486
|- style="text-align:center;"
|
| 8968
|- style="text-align:center;"
|
| 6335
|- style="text-align:center;"
|
| 7633
|- style="text-align:center;"
|
| 8496
|}
</center>

[[Category: OR/15/070 Quantification of phytic acid in grains | 11]]

OR/15/070 Appendix 3 - Revision history

Dbk: 1 revision imported

Ajhil at 09:31, 31 August 2016